Methyl Benzenesulfonate CAS 80-18-2 Purity >99.0% (GC) High Quality

Short Description:

Chemical Name: Methyl Benzenesulfonate

Synonyms: Benzenesulfonic Acid Methyl Ester

CAS: 80-18-2

Purity: >99.0% (GC)

Appearance: Colorless to Slightly Pale Yellow Liquid

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80-18-2 - Description:

Shanghai Ruifu Chemical Co., Ltd. is the leading manufacturer and supplier of Methyl Benzenesulfonate (CAS: 80-18-2) with high quality, commercial production. We can provide Certificate of Analysis (COA), Safety Data Sheet (SDS), worldwide delivery, small and bulk quantities available, strong after-sale service. Welcome to order. Please contact: alvin@ruifuchem.com

80-18-2 - Chemical Properties:

Chemical Name	Methyl Benzenesulfonate
Synonyms	Benzenesulfonic Acid Methyl Ester; Methyl Benzenesulphonate; Methyl Besylate; Methyl Ester of Benzenesulphonic Acid
CAS Number	80-18-2
Stock Status	In Stock, Production Scale Up to Tons
Molecular Formula	C7H8O3S
Molecular Weight	172.20
Melting Point	-4℃
Boiling Point	280℃
Flash Point	143℃
Specific Gravity (20/20)	1.2730g/ml
Refractive Index	1.52
Sensitive	Moisture Sensitive
Solubility	Insoluble in Water. Soluble in Ethanol, Ether, Chloroform
COA & MSDS	Available
Free Sample	Available
Brand	Ruifu Chemical

80-18-2 - Specifications:

Item	Specifications	Results
Appearance	Colorless to Slightly Pale Yellow Liquid	Complies
Purity / Analysis Method	>99.0% (GC)	99.61%
Water (K.F)	<0.50%	0.25%
Refractive Index n20/D	1.516~1.518	Complies
Benzenesulfonic Acid	<0.20%	<0.20%
Benzenesulfonyl Chloride	<0.20%	<0.20%
Solubility	Insoluble in Water; Freely Souble in Ethanol, Ether	Complies
1 H NMR Spectrum	Consistent With Structure	Complies
Test Standard	Enterprise Standard	Complies

Package & Storage:

Package: 25kg/Barrel, 200kg/Plastic Drum, or according to customer's requirement.

Storage Condition: Store in sealed containers at cool and dry place; Protect from light and moisture.

80-18-2 - Synthetic Route:

80-18-2 - Synthetic Procedure
(1) Add Benzenesulfonyl Chloride (CAS: 98-09-9) and Methanol into 500L reactor, and then drop sodium hydroxide solution when the temperature drops below 10 degrees. After the drip is finished, the tower rises to room temperature and reacts for 4 hours.
(2) Wash to remove salt and collect the underlying organic phase.
(3) Add the product of the above step to 500L reactor and add methanol and sodium hydroxide solution for 8 hours at room temperature.
(4) Repeat (2)
(5) The product is purified after three times of refining.

80-18-2 - Analysis Method:

Water: Water by Karl Fischer: <0.50%
Density: The relative density measured by gravity bottle is 1.2730g/ml
Purity: >99.0% (GC)
Chromatographic Column: SE-30
Detector: FID
Column Temperature: 150℃ (for 5min), 10℃/min increased to 280℃ for 15min.
Vaporization Temperature: 230℃
Detection Temperature: 280℃

Advantages:

FAQ:

80-18-2 - Risk and Safety:

Risk Codes R34 - Causes burns
R22 - Harmful if swallowed
R43 - May cause sensitization by skin contact
Safety Description S28A -
S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection.
UN IDs 3265
WGK Germany 3
RTECS DB7151000
TSCA Yes
HS Code 2904100000
Hazard Note Irritant/Corrosive
Hazard Class 8
Packing Group III

80-18-2 - Application:

Methyl Benzenesulfonate (CAS: 80-18-2) is used as a raw material for the dye and pharmaceutical industries, used as an alkylating agent in organic synthesis for the production of some synthetic dye. It can also be used for the manufacturing the thin-cation exchanger film. Methyl benzenesulfonate is the effective methylating reagent of synthetic multiple organic intermediate.

80-18-2 - Safety:

Methyl Benzenesulfonate, Extremely toxic! Its vapor irritates eyes, mucous membranes and skin, can cause sensitization and dermatitis, and direct contact is strictly prohibited. Production equipment should be sealed to prevent leakage. The operator should wear protective gear. Flush with plenty of water when splash and skin.
Storage and Transportation shall be carried out according to the regulations for flammable and extremely toxic substances.