N-Phenylglycine CAS 103-01-5 H-DL-Phg-OH Purity >99.0% (HPLC) Factory

Short Description:

Chemical Name: N-Phenylglycine

Synonyms: H-DL-Phg-OH 

CAS: 103-01-5

Purity: >99.0% (HPLC)

Appearance: Pale Yellow to Yellow Powder

Unnatural Amino Acids Derivatives, High Quality

Contact: Dr. Alvin Huang

Mobile/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com


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Description:

Shanghai Ruifu Chemical Co., Ltd. is the leading manufacturer of N-Phenylglycine (H-DL-Phg-OH) (CAS: 103-01-5) with high quality. Ruifu supplys a series of amino acids. We can provide worldwide delivery, competitive price, small and bulk quantities available. Purchase N-Phenylglycine, Please contact: alvin@ruifuchem.com

Chemical Properties:

Chemical Name N-Phenylglycine 
Synonyms H-DL-Phg-OH; H-DL-Phenylglycine; Anilinoacetic Acid; Phenylglycine; DL-Phenylglycine; DL-Alpha-Phenylglycine; DL-α-Phenylglycine; (Phenylamino)acetic Acid; Nα-Aminophenylacetic Acid
Stock Status In Stock 
CAS Number 103-01-5
Molecular Formula C8H9NO2
Molecular Weight 151.17 g/mol
Melting Point 121.0~123.0℃(lit.)
Sensitive Light Sensitive, Air Sensitive 
Water Solubility  Moderately Soluble in Water
Solubility in Methanol  Almost Transparency
Storage Temp.  Cool & Dry Place (2~8℃) 
COA & MSDS Available
Category   Unnatural Amino Acids Derivatives  
Brand Ruifu Chemical

Specifications:

Items Inspection Standards Results
Appearance Pale Yellow to Yellow Powder Complies      
Melting Point 121.0~123.0℃ Complies 
Loss on Drying <0.50% 0.17% 
Residue on Ignition <0.20% 0.05%
Purity / Analysis Method >99.0% (HPLC)  99.76% 
Infrared Spectrum Consistent with Structure  Complies      
1 H NMR Spectrum Consistent with Structure Complies      
Conclusion The product has been tested & complies with the specifications

Package/Storage/Shipping:

Package: Bottle, Aluminium foil bag, 25kg/Cardboard Drum, or according to customer's requirement.
Storage Condition: Store in sealed containers at cool and dry (2~8℃) warehouse away from incompatible substances. Protect from light and moisture.
Shipping: Deliver to worldwide by FedEx / DHL Express. Provide fast and reliable delivery. 

Advantages:

Sufficient Capacity: Sufficient facilities and technicians

Professional Service: One stop purchasing service

OEM Package: Custom package and label available

Fast Delivery: If within stock, three days delivery guaranteed

Stable Supply: Maintain reasonable stock    

Technical Support: Technology solution available

Custom Synthesis Service: Ranged from grams to kilos

High Quality: Established a complete quality assurance system

FAQ:

How to Purchase? Please contact Dr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com 

15 Years Experience? We have more than 15 years of experience in the manufacture and export of a wide range of high quality pharmaceutical intermediates or fine chemicals.

Main Markets? Sell to domestic market, North America, Europe, India, Korea, Japanese, Australia, etc.

Advantages? Superior quality, affordable price, professional services and technical support, fast delivery.

Quality AssuranceStrict quality control system. Professional equipment for analysis include NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, K.F, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, etc.

SamplesMost products provide free samples for quality evaluation, shipping cost should be paid by customers.

Factory AuditFactory audit welcome. Please make an appointment in advance.

MOQ? No MOQ. Small order is acceptable.

Delivery Time? If within stock, three days delivery guaranteed.

TransportationBy Express (FedEx, DHL), by Air, by Sea.

Documents? After sales service: COA, MOA, ROS, MSDS, etc. can be provided.

Custom SynthesisCan provide custom synthesis services to best fit your research needs.

Payment TermsProforma invoice will be sent first after confirmation of order, enclosed our bank information. Payment by T/T (Telex Transfer), PayPal, Western Union, etc. 

103-01-5 - Risk and Safety:

Risk Codes
R11 - Highly Flammable
R34 - Causes burns
Safety Description
S24/25 - Avoid contact with skin and eyes.
S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection.
S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S16 - Keep away from sources of ignition.
WGK Germany 3
TSCA Yes
HS Code 2922491990

Application:

N-Phenylglycine (H-DL-Phg-OH) (CAS: 103-01-5) is a derivative of Glycine. A glycine carrying an N-phenyl substituent. For the manufacture of L-Phenylglycine; For the manufacture of indigo dyes, used as pharmaceutical intermediates. Intermediates of Cephalexin and Cefaclor.
N-Phenylglycine can be used in peptide synthesis, reaction type solution phase peptide synthesis. N-Phenylglycine can be also used as an organic synthesis intermediate, pharmaceutical intermediate, biochemical reagent or chemical reagent.
Production method Benzaldehyde is cyclized, hydrolyzed and neutralized to obtain the product. Put the solution of ammonia bicarbonate and sodium cyanide into the reaction pot, drip benzaldehyde under stirring, and heat preservation at 75-80℃ for 3 hours to obtain phenylhydantoin. Pump into an autoclave, add sodium hydroxide solution, raise the temperature, empty the ammonia gas generated by the reaction for 1h, and then hydrolyze at 130-160℃ for 3h. Feeding, adding HCl to neutralize until pH = 6-7, centrifugally spin dry to obtain DL-2-Phenylglycine. There is also a glyoxylic acid route, which can reduce production costs and solve the problem of high toxicity of traditional process raw materials.  

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