Boc-β-Iodo-Ala-OMe CAS 93267-04-0 Purity >99.0% (HPLC) Factory

Short Description:

N-Boc-3-Iodo-L-Alanine Methyl Ester

Synonyms: Boc-β-Iodo-Ala-OMe

CAS: 93267-04-0

Purity: >99.0% (HPLC)

Appearance: White to Light Yellow Crystals

Boc-Amino Acids, High Quality

Contact: Dr. Alvin Huang

Mobile/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com

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Product Detail

Product Tags

Description:

Shanghai Ruifu Chemical Co., Ltd. is the leading manufacturer of N-Boc-3-Iodo-L-Alanine Methyl Ester (Boc-β-Iodo-Ala-OMe) (CAS: 93267-04-0) with high quality. Ruifu Chemical supplys a series of amino acids and derivatives. We can provide worldwide delivery, small and bulk quantities available. Purchase Boc-β-Iodo-Ala-OMe, Please contact: alvin@ruifuchem.com

Chemical Properties:

Chemical Name	N-Boc-3-Iodo-L-Alanine Methyl Ester
Synonyms	Boc-β-Iodo-Ala-OMe; Boc-Ala(3-I)-OMe; Boc-Beta-Iodo-Ala-OMe; (R)-Boc-β-Iodo-Ala-Ome; N-(tert-Butoxycarbonyl)-3-Iodo-L-Alanine Methyl Ester; L-N-Boc-3-Iodoalanine Methyl Ester
Stock Status	In Stock
CAS Number	93267-04-0
Molecular Formula	C9H16INO4
Molecular Weight	329.13 g/mol
Melting Point	45.0~55.0℃ (lit.)
Density	1.551±0.06 g/cm3
Sensitive	Light Sensitive, Heat Sensitive
Solubility	Soluble in Methanol
Storage Temp.	Cool & Dry Place (≤4℃)
COA & MSDS	Available
Category	Boc-Amino Acids
Brand	Ruifu Chemical

Safety Information:

Safety Statements	24/25 - Avoid contact with skin and eyes.	F	8
WGK Germany	3	HS Code	2922491990

Specifications:

Items	Inspection Standards	Results
Appearance	White to Light Yellow Crystals	Complies
Melting Point	45.0~55.0℃	47.6~48.6℃
Specific Rotation [α]20/D	-4.0° ± 1.0° (C=2 in MeOH)	-4.4°
Clarity of Solution	0.3 gram in 2ml MeOH Clear Solution	Complies
Water Content (K.F.)	<1.00%	0.18%
Purity / Analysis Method	>99.0% (HPLC)	99.47%
IR Spectrum	In Accordance With the Standard	Complies
NMR Spectrum	In Accordance With the Standard	Complies
Conclusion	This Product by Inspection Accords with the Enterprise Standard
Main Uses	Boc-Amino Acids; Peptide Synthesis; Pharmaceutical Intermediates

Package & Storage:

Package: Fluorinated Bottle, Aluminium foil bag, 25kg/Cardboard Drum, or according to customer's requirement.

Storage Condition: Store in sealed containers at cool, dry (≤4℃) warehouse away from incompatible substances. Protect from light, heat and moisture. Store away from oxidizing agent.

Advantages:

Sufficient Capacity: Sufficient facilities and technicians

Professional Service: One stop purchasing service

OEM Package: Custom package and label available

Fast Delivery: If within stock, three days delivery guaranteed

Stable Supply: Maintain reasonable stock

Technical Support: Technology solution available

Custom Synthesis Service: Ranged from grams to kilos

High Quality: Established a complete quality assurance system

FAQ:

How to Purchase? Please contact Dr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com

15 Years Experience? We have more than 15 years of experience in the manufacture and export of a wide range of high quality pharmaceutical intermediates or fine chemicals.

Main Markets? Sell to domestic market, North America, Europe, India, Korea, Japanese, Australia, etc.

Advantages? Superior quality, affordable price, professional services and technical support, fast delivery.

Quality Assurance? Strict quality control system. Professional equipment for analysis include NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, K.F, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, etc.

Samples? Most products provide free samples for quality evaluation, shipping cost should be paid by customers.

Factory Audit? Factory audit welcome. Please make an appointment in advance.

MOQ? No MOQ. Small order is acceptable.

Delivery Time? If within stock, three days delivery guaranteed.

Transportation? By Express (FedEx, DHL), by Air, by Sea.

Documents? After sales service: COA, MOA, ROS, MSDS, etc. can be provided.

Custom Synthesis? Can provide custom synthesis services to best fit your research needs.

Payment Terms? Proforma invoice will be sent first after confirmation of order, enclosed our bank information. Payment by T/T (Telex Transfer), PayPal, Western Union, etc.

Application:

N-Boc-3-Iodo-L-Alanine Methyl Ester (Boc-β-Iodo-Ala-OMe) (CAS: 93267-04-0), Boc-amino acids, peptide synthesis, organic synthesis intermediate, pharmaceutical intermediates, biochemical reagents. Boc-β-Iodo-Ala-OMe is an organic intermediate, which can be obtained by reacting with elemental iodine Boc-L-serine methyl ester as raw material. Boc-L-serine methyl ester (20g,91mmol) is dissolved in THF(400mL) and cooled in an ice water bath. Triphenylphosphine (36g,137mmol) and pyridine (14g,177mmol) were added to the upper solution in turn, and then I2(34g,134mmol) was added in batches to maintain the temperature below 20 ℃ for 4 hours. After the reaction is completed, add ice water to the reaction solution to quench the reaction and extract it with ether. The organic phase obtained was washed with 1% hydrochloric acid, 5% Na2SO3 solution and saturated NaCl solution, dried with anhydrous Na2SO4, and concentrated after filtration. The resulting residue is added to petroleum ether, stirred to precipitate solids, filtered, and the filter residue is washed with petroleum ether. The filtrate was concentrated to get 26g of white or yellowish solid with 87% yield.