Phenylhydrazine CAS 100-63-0 Purity >99.0% (GC)

Short Description:

Chemical Name: Phenylhydrazine 

CAS: 100-63-0

Purity: >99.0% (GC) 

Appearance: Colorless to Light Yellow Oily Liquid 

High Quality, Commercial Production

Contact: Dr. Alvin Huang

Mobile/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com


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100-63-0 - Description:

Shanghai Ruifu Chemical Co., Ltd. is the leading manufacturer and supplier of Phenylhydrazine (CAS: 100-63-0) with high quality. We can provide COA, worldwide delivery, small and bulk quantities available. If you are interested in this product, please send detailed information includes CAS number, product name, quantity to us. Please contact: alvin@ruifuchem.com

100-63-0 - Chemical Properties:

Chemical Name Phenylhydrazine 
Synonyms Hydrazinobenzene; Monophenylhydrazine; 1-Hydrazinobenzene; Phenyl Hydrazide; PhNHNH2 
CAS Number 100-63-0
Stock Status In Stock, Production Capacity 30 Tons per Month  
Molecular Formula C6H8N2 
Molecular Weight 108.14  
Melting Point 18.0~21.0℃(lit.)
Boiling Point 238.0~241.0℃(lit.)
Sensitive Light Sensitive, Air Sensitive 
Solubility in Water Soluble in Water, 145 g/L (20℃)
Solubility Miscible With Ether, Benzene, Alcohol, Chloroform. Very Soluble in Acetone
Stability Stable, but May Decompose in Sunlight. May be Air or Light Sensitive. Incompatible With Strong Oxidizing Agents, Metal Oxides.
Storage Temp. Store at Room Temperature
COA & MSDS Available
Origin of Product   China
Brand Ruifu Chemical

100-63-0 - Specifications:

Item Specifications Results
Appearance Colorless to Light Yellow Oily Liquid Conforms                         
Phenylhydrazine Purity  >99.0% (GC) 99.56% 
Crystallization Point ~19.0℃ 19.4℃ 
Ash <0.20% 0.09% 
Aniline <0.50% 0.17% 
Benzene <0.30% 0.07% 
Water by Karl Fischer <0.30% 0.09% 
Refractive Index n20/D 1.606~1.610 Conforms  
Density (20℃) 1.098~1.102 Conforms  
Infrared Spectrum Conforms to Structure Conforms  
Proton NMR Spectrum Conforms to Structure Conforms  
Conclusion The product has been tested and complies with the given specifications
Note: This product is low melting point, may change state in different environments (solid, liquid or semi-solid)

100-63-0 - Package & Storage:

Package: Fluorinated Bottle, 25kg/Drum, 200kg/Drum or according to customer's requirement

Storage Condition: Air and light sensitive. Keep the container tightly closed in a dry and well-ventilated place. Incompatible with oxidizing agents.

100-63-0 - Chromatographic Conditions:

- Column: Agilent hc-C18 (150×4.6mm, 5μm);
- Mobile Phase: methanol-water (volume ratio 40:60), containing 0.02mol/L antioxidant, 0.02mol/L modifier (M), 0.02mol/L K2HPO2-KH2PO2, and adjusted to pH=5 with H3PO4;
- Flow Rate: 1.0mL/min;
- Sample Size: 20μL;
- Detection Wavelength: 272nm.

Advantages:

Sufficient Capacity: Sufficient facilities and technicians

Professional Service: One stop purchasing service

OEM Package: Custom package and label available

Fast Delivery: If within stock, three days delivery guaranteed

Stable Supply: Maintain reasonable stock    

Technical Support: Technology solution available

Custom Synthesis Service: Ranged from grams to kilos

High Quality: Established a complete quality assurance system

100-63-0 - FAQ:

How to Purchase? Please contact Dr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com 

15 Years Experience? We have more than 15 years of experience in the manufacture and export of a wide range of high quality pharmaceutical intermediates or fine chemicals.

Main Markets? Sell to domestic market, North America, Europe, India, Korea, Japanese, Australia, etc.

Advantages? Superior quality, affordable price, professional services and technical support, fast delivery.

Quality AssuranceStrict quality control system. Professional equipment for analysis include NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, K.F, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, etc.

SamplesMost products provide free samples for quality evaluation, shipping cost should be paid by customers.

Factory AuditFactory audit welcome. Please make an appointment in advance.

MOQ? No MOQ. Small order is acceptable.

Delivery Time? If within stock, three days delivery guaranteed.

TransportationBy Express (FedEx, DHL), by Air, by Sea.

Documents? After sales service: COA, MOA, ROS, MSDS, etc. can be provided.

Custom SynthesisCan provide custom synthesis services to best fit your research needs.

Payment TermsProforma invoice will be sent first after confirmation of order, enclosed our bank information. Payment by T/T (Telex Transfer), PayPal, Western Union, etc. 

100-63-0 - Risk and Safety:

Risk Codes R45 - May cause cancer
R23/24/25 - Toxic by inhalation, in contact with skin and if swallowed.
R36/38 - Irritating to eyes and skin.
R43 - May cause sensitization by skin contact
R48/23/24/25 -
R50 - Very Toxic to aquatic organisms
R68 - Possible risk of irreversible effects
Safety Description S53 - Avoid exposure - obtain special instructions before use.
S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
S61 - Avoid release to the environment. Refer to special instructions / safety data sheets.
UN IDs UN 2572 6.1/PG 2
WGK Germany 3
RTECS MV8925000
FLUKA BRAND F CODES 8-10-23
TSCA Yes
HS Code 2928000090
Hazard Class 6.1
Packing Group II
Toxicity LD50 orally in Rabbit: 188 mg/kg

100-63-0 - Application:

Phenylhydrazine (CAS: 100-63-0), is also known as the Hydrazinobenzene. It was first successfully synthesized by the German organic chemist Hermann-Emil-Fischer in 1875 and is the first synthesized hydrazine derivatives. It can be easily subject to oxidization in the air and exhibit dark brown or dark red.
Phenylhydrazine can often be used as intermediates of organic dyes, pharmaceuticals and pesticide. Phenylhydrazine can also be used as organic intermediates for synthesis of pyrazoline, triazole, and indole; Phenylhydrazine can also be used as dye intermediates; Phenylhydrazine can also be used as pharmaceutical intermediates for preparation of antipyretic, analgesic, anti-inflammatory drugs such as antipyrine and aminopyrine, etc; it can also be used as photography drugs (photosensitive dye); Phenylhydrazine is also the raw material for the production of pesticides; Phenylhydrazine is used as a stabilizer for explosives; as a reagent for aldehydes, ketones and sugars in chemical analysis; Phenylhydrazine is involved in Fischer indole synthesis to prepare indoles, which find application as intermediates in the pharmaceuticals particularly for the tryptamine drug. It is used as an N-protecting reagent and for cleavage of phthaloyl group. Phenylhydrazine is also used as an analytical reagent. Phenylhydrazine is also an important reagent for identification of carbonyl group and can be used for identifying aldehydes, ketones and carbohydrates.
Common method of its preparation is through the reaction between aniline and sodium nitrite under the action of hydrochloric acid for generation of diazonium salt which is then reduced by sulfite/sodium reduction for obtaining it. Acid precipitation can generate phenylhydrazine hydrochloride with neutralization generating phenylhydrazine. 

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